Stirred Autoclave High Pressure Reactor 50ml-250ml

Salient Features

  • High pressure autoclaves for chemical reactions like hydrogenation, oxidation, alkylation, chlorination. carboxylation, nitration, polymerization, amination, bromination,ethoxylation, esterification, sulphonation etc.
  • 50 ml to 100 liters volume
  • Pressures upto 350 bar & temperatures upto 500°C
  • Available in different Material of Constructions (MOC) like SS-316, SS-316L, Hastelloy B/C, Monel, Nickel, Inconel, Titanium, Tantalum, Zirconium
  • High torque zero leakage magnetic drive coupling
  • Ex-proof / CE / PED / ASME / UL / CSA certified systems on request
  • Fully automated PC controlled high pressure system / pilot plant to continuously monitor, control & record various parameters like temperature, pressure, motor speed, gas / liquid flow, level, pH, ORP, DO, IR, turbidity, torque etc.

Standard models for 50 ml High Pressure Autoclaves

Model no.A 1213A 1215A 1223A 1225A 1233A 1235
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)404040404040
Vessel Internal Height (mm)636363636363
Min. Stirrable Volume (ml)202020202020

Standard models for 100 ml High Pressure Autoclaves

Model no.A 1313A 1315A 1323A 1325A 1333A 1335
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)404040404040
Vessel Internal Height (mm)838383838383
Min. Stirrable Volume (ml)202020202020

Standard models for 250 ml High Pressure Autoclaves

Model no.A 1413A 1415A 1423A 1425A 1433A 1435
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)656565656565
Vessel Internal Height (mm)808080808080
Min. Stirrable Volume (ml)505050505050

Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress value & maximum allowable temperature as per ASME code.

Technical specification for High Pressure Autoclaves standard models

Sr. Description Specification
A Material of Construction SS 316 wetted parts
B Head Mounting Style Removable head and vessel design
C Heating Type Electrical ceramic band heater with cladding & insulation & heater temperature control for 500°C
D Motor ⅛ hp AC motor with 100-1450 RPM
E Shaft Sealing Zero leakage magnetic drive coupling M20 with 2 Nm torque
F Stirrer 4 bladed turbine stirrer
G Standard Nozzles, Valves & Fittings External Valves & Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, solenoid valve at inlet of cooling coil, vent needle valve (All needle valves ⅛" size)
Internal Fittings:
Serpentine cooling coil, dip tube, thermowell with RTD PT100 temperature sensor
H Gasket PTFE up to 300°C and metallic grafoil gasket up to 500°C
I Closure Type Split clamp with clamp bolts
J Control Panel SS control panel with programmable PID temperature controller with high temperature alarm and variable frequency drive for motor speed control
K Power Supply 1Ø, 220 V AC, 50 / 60 Hz
L Mounting & Dimensions Mounting Description Dimensions in mm
Width Depth Height
SS Table Top Reactor 240 310 800
SS Table Top Control Panel 275 275 300

Enquiry guide for 50 ml, 100 ml & 250 ml customized high pressure autoclaves models

Enquiry code structure is Standard Model no-A-B-C-D2-D3-E-F-I-J-L-M where A, B, C, D2, D3, E, F, I, J, L & M options can be selected from below tables. The below options will be in place of standard supply. For example 100 ml, 100 bar, 300°C, Hastelloy C, fixed head autoclave with ATEX Zone1 certified, heater, motor & panel will read as A 1313-HC6-K-EZ-AZ-ATP

A Material of Construction
SS 316L 316L
Hastelloy C 276 HC6
Hastelloy C 22 HC2
Hastelloy B HB
Monel 400 MN4
Inconel 600 IN6
Inconel 625 IN5
Nickel 200 NK2
Titanium Gr. 2 TI2
Zirconium 702 ZR7
Tantalum TAN
B Head Mounting Style
Fixed head with manual vessel raising lowering K
C Heating Style
Electrical ex-proof, IIB + H2 certified EA
Electrical ex-proof ATEX Zone1 certified EZ
Electrical ex-proof Class 1 Div 2 EC
Welded SS 304 jacket with insulation JS
Welded SS 304 jacket with electrical ceramic heater JH
Peltier cooler for -25 to 150°C PL
D2 Motor RPM
Upto 3000 rpm RT
D3 Motor Type
¼ hp ex-proof gas group IIB (Zone 1) XB
¼ hp ex-proof gas group IIC (Zone 1) XC
¼ hp ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ
¼ hp ex-proof CSA certified Class 1 Div 2 group A, B, C, D CD
⅛ hp compact in-line brushless DC motor BD
E Mag Drive Torque
2 Nm 20
F Stirrer Options*
Hollow shaft with gas induction Impeller SH
Ruston turbine SR
Paddle SD
Propeller SP
I Closure Type
Threaded cap with FKM (Viton)'O' ring up to 225°C CV
Threaded cap with FFKM (Kalrez) 'O' ring up to 275°C CK
J Control Panel
Ex-proof gas group IIA/IIB zone 1 certified F2B
Ex-proof gas group IIC zone 1 certified F2C
Ex-proof ATEX zone 1 certified ATP
Ex-proof class 1 div. 2 certified C12
Touch screen TSP
L Mounting & Overall Dimensions (WxDxH)
Trolley 1010 mm x 410 mm x 1300 mm TL
M Certifications***
Design approval as per ASME code by notified body DAC
CE-PED 2014/68/EU PED
ASME U/U2 stamp coded ASU
ATEX certified reactor 2014/34/EU ASA
CE marked panel & electrical parts ECE
UL/CSA marked panel & electrical parts USC
Notes:
  1. Customer is advised to select best suited options for most optimized price & delivery.
  2. For other optional accessories please refer Accessories tab
  3. All above options may not be available / possible with all models.
  4. Customization of volume, material, pressure, temperature etc. may be possible on request.
  5. Different power supply options may be possible on request.
  6. Overall dimensions are indicative, they may change depending on the optional accessories or specific design modifications opted.
  7. * Stirrer options can be in place of standard or additional multiple interchangeable.
  8. ** Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.

Lab Autoclaves Optional Accessories

MAGNA-SAFE INTERNATIONAL
P.O.BOX 447
OLD BRIDGE, NJ 08857-0447

 ( 866 ) 626 8885

  www.magnasafe.com

Get In Touch

Fill the from given below to get in touch with us. we will get back to you soon!