Stirred Autoclave High Pressure Reactor 10ltr-100ltr

Salient Features

  • High pressure autoclaves for chemical reactions like hydrogenation, oxidation, alkylation, chlorination. carboxylation, nitration, polymerization, amination, bromination,ethoxylation, esterification, sulphonation etc.
  • 50 ml to 100 liters volume
  • Pressures upto 350 bar & temperatures upto 500°C
  • Available in different Material of Constructions (MOC) like SS-316, SS-316L, Hastelloy B/C, Monel, Nickel, Inconel, Titanium, Tantalum, Zirconium
  • High torque zero leakage magnetic drive coupling
  • Ex-proof / CE / PED / ASME / UL / CSA certified systems on request
  • Fully automated PC controlled high pressure system / pilot plant to continuously monitor, control & record various parameters like temperature, pressure, motor speed, gas / liquid flow, level, pH, ORP, DO, IR, turbidity, torque etc.

Standard models for 10 ltr High Pressure Autoclaves

Model no.A 3113A 3115A 3123A 3125A 3133A 3135
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)183183183183183183
Vessel Internal Height (mm)420420420420420420
Min. Stirrable Volume (ltr)111111

Standard models for 20 ltr High Pressure Autoclaves

Model no.A 3213A 3215A 3223A 3225
Design Pressure100 bar100 bar200 bar200 bar
Design Temperature300°C 500°C300°C 500°C
Vessel I/D (mm)248248248248
Vessel Internal Height (mm)495495495495
Min. Stirrable Volume (ltr)2.62.62.62.6

Standard models for 25 ltr High Pressure Autoclaves

Model no.A 3313A 3315A 3323A 3325
Design Pressure100 bar100 bar200 bar200 bar
Design Temperature300°C 500°C300°C 500°C
Vessel I/D (mm)248248248248
Vessel Internal Height (mm)595595595595
Min. Stirrable Volume (ltr)2.62.62.62.6

Standard models for 50 ltr High Pressure Autoclaves

Model no.A 3403A 3405A 3413A 3415
Design Pressure50 bar50 bar100 bar100 bar
Design Temperature300°C 500°C300°C 500°C
Vessel I/D (mm)355355343343
Vessel Internal Height (mm)558558600600
Min. Stirrable Volume (ltr)6666

Standard models for 100 ltr High Pressure Autoclaves

Model no.A 3503A 3505A 3513A 3515
Design Pressure50 bar50 bar100 bar100 bar
Design Temperature300°C 500°C300°C 500°C
Vessel I/D (mm)456456440440
Vessel Internal Height (mm)699699735735
Min. Stirrable Volume (ltr)12121212

Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress value & maximum allowable temperature as per ASME code.

Technical specification for High Pressure Autoclaves standard models

Sr. Description Specification
A Material of Construction SS 316 wetted parts
B Head Mounting Style Removable head and vessel design
C Heating Type Electrical ceramic band heater with cladding & insulation & heater temperature control for 500°C
D Motor ¼ hp AC motor for 10 ltr, 20 ltr & 25 ltr locked to 750 rpm
½ hp AC motor for 50 ltr & 100 ltr locked to 500 rpm
E Shaft Sealing Zero leakage magnetic drive coupling M20 with 2 Nm torque
F Stirrer 2 stage 6 bladed turbine stirrer
G Standard Nozzles, Valves & Fittings External Valves & Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, vent needle valve, ball valve for powder/liquid inlet with funnel, flush bottom valve
Internal Fittings:
Helical cooling coil, dip tube, thermowell with RTD PT100 temperature sensor
H Gasket PTFE up to 300°C and metallic grafoil gasket up to 500°C
I Closure Type Split clamp with clamp bolts
J Control Panel SS control panel with programmable PID temperature controller with high temperature alarm and variable frequency drive for motor speed control
K Power Supply 1Ø, 220 V AC, 20 amp, 50 / 60 Hz for 10 ltr
3Ø, 440 V AC, 25 amp, 50 / 60 Hz for 20 ltr to 100 ltr
L Mounting & Dimensions Mounting Reactor Volume Dimensions with control panel in mm
Width Depth Height
SS Trolley 10 ltr 1310 585 1550
SS Trolley 20 ltr 1310 585 1700
SS Trolley 25 ltr 1310 585 1800
SS Trolley 50 ltr 1500 675 2350
SS Trolley 100 ltr 1500 780 2350

Enquiry guide for 10 ltr, 20 ltr, 25 ltr, 50 ltr & 100 ltr customized high pressure autoclaves models

Enquiry code structure is Standard Model no-A-B-C-D1-D2-D3-E-F-G-I-J-L-M where A, B, C, D1, D2, D3, E, F, G, I, J, L & M options can be selected from below tables. The below options will be in place of standard supply. For example 100 ml, 100 bar, 300°C, Hastelloy C, fixed head autoclave with ATEX Zone1 certified, heater, motor & panel will read as A 1313-HC6-K-EZ-AZ-ATP

A Material of Construction
SS 316L 316L
Hastelloy C 276 HC6
Hastelloy C 22 HC2
Hastelloy B HB
Monel 400 MN4
Inconel 600 IN6
Inconel 625 IN5
Nickel 200 NK2
Titanium Gr. 2 TI2
Zirconium 702 ZR7
Tantalum lined TNL
B Head Mounting Style
Fixed head with pneumatic vessel raising lowering (10 ltr to 25 ltr) P
Fixed head with hydraulic vessel raising lowering (50 ltr & 100 ltr) H
Fixed head with pneumatic vessel raising lowering & tilting (10 ltr to 25 ltr) PT
Fixed head with hydraulic vessel raising lowering & tilting (50 ltr & 100 ltr) HT
C Heating Style
Electrical ex-proof, IIB + H2 certified EA
Electrical ex-proof ATEX Zone1 certified EZ
Electrical ex-proof Class 1 Div 2 EC
Welded SS 304 jacket with insulation JS
Welded SS 304 jacket with electrical ceramic heater JH
Limpet coil SS 304 with insulation (20 ltr to 100 ltr) LC
D1 Motor HP
1 hp H10
2 hp H20
3 hp H30
D2 Motor RPM
Gear box upto 440 rpm R4
D3 Motor Type
Ex-proof gas group IIB (Zone 1) XB
Ex-proof gas group IIC (Zone 1) XC
Ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ
Ex-proof CSA certified Class 1 Div 2 group A, B, C, D CD
¼ hp compact in-line brushless DC motor QD
E Mag Drive Torque
12 Nm (for 10 to 25 ltr) M120
20 Nm (upto 750 rpm, for 10 to 25 ltr) M200
40 Nm (upto 750 rpm) M400
F Stirrer Options*
Hollow shaft with gas induction Impeller SH
Anchor (Serpentine cooling coil, max 100 rpm) SA
Spiral (No cooling coil, max 100 rpm) SS
Ruston turbine SR
Paddle SD
Propeller SP
G Valves & Fittings
Serpentine cooling coil SCC
J Control Panel
Ex-proof gas group IIA/IIB zone 1 certified F2B
Ex-proof gas group IIC zone 1 certified F2C
Ex-proof ATEX zone 1 certified ATP
Ex-proof class 1 div. 2 certified C12
Touch screen TSP
L Mounting & Overall Dimensions (WxDxH) in mm
Mounting Volume Reactor size Panel size Code
Floor Stand 10 ltr 585 X 560 X 1550 275 X 275 X 300 FS
20 ltr 585 X 560 X 1700 400 X 380 X 340
25 ltr 585 X 560 X 1800
50 ltr 675 X 675 X 2350
100 ltr 780 X 780 X 2350
M Certifications**
Design approval as per ASME code by notified body DAC
CE-PED 2014/68/EU PED
ASME U/U2 stamp coded ASU
ATEX certified reactor 2014/34/EU ASA
CE marked panel & electrical parts ECE
UL/CSA marked panel & electrical parts USC
Notes:
  1. Customer is advised to select best suited options for most optimized price & delivery.
  2. For other optional accessories please refer Accessories tab
  3. All above options may not be available / possible with all models.
  4. Customization of volume, material, pressure, temperature etc. may be possible on request.
  5. Different power supply options may be possible on request.
  6. Overall dimensions are indicative, they may change depending on the optional accessories or specific design modifications opted.
  7. * Stirrer options can be in place of standard or additional multiple interchangeable.

Lab Autoclaves Optional Accessories

MAGNA-SAFE INTERNATIONAL
P.O.BOX 447
OLD BRIDGE, NJ 08857-0447

 ( 866 ) 626 8885

  www.magnasafe.com

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